2O2 JOURNAL OF THE SOCIETY OF COSMETIC CHEMISTS (1 mil = 10 -a inch). Its use is mandatory for measuring resistance to sag in some US Federal Specifications. Description andprocedure. For use on dentifrices, a simplified sag meter in the range 60-120 mils was constructed (Fig. 13). The brass doctor blade has 11 notches, each 1/4 in. wide with intervening gaps of 1/16 in. The heights of the notches are 60, 70, 80, 90, 100, 120, 140, 160, 180 and 200 mils. The last notch is a thin, shallow marker. Toothpaste is placed upon a horizontal, glazed glass plate along the recessed side of the meter, which is drawn at a slow, steady rate along a straight edge. A series of equidistant, parallel stripes of uniform width and varying heights is obtained. The plate is placed in a vertical position with the stripes horizontal, the fattest stripes being lowest. A slightly roughened surface is required to prevent slip of the stripes of toothpaste. Results. Fig. 14 shows the results of a typical sag test. The five fattest stripes have sagged, obscuring the intervening gaps. (The lowest stripe is the shallow marker.) The sag number is therefore 5. A series of pastes can be compared easily in this way, sag ceasing after about 30 min. For a series of more fluid pastes, the time taken for the most mobile one to show a sag number of 1 may be noted. The other pastes can then be ranked in order of sag number, using the same time span. Fig. 15 illus- strates the good reproducibility of the test. Each horizontal line shows the I o I 200 I 400 Time (s) I I I 600 I 800 Figure 15. Span results for five trials on one paste. Final sag number for all trials 5.
JOURNAL OF THE SOCIETY OF COSMETIC CHEMISTS .: Figure 13. The toothpaste sag meter. Facing page 202
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