NEW FRAGRANCES FROM 2-METHYLFURAN: I 97
98 JOURNAL OF COSMETIC SCIENCE layer was extracted with toluene (50 ccm). The organic layer was washed to a neutral pH value and dried with anhydrous MgSO 4. After evaporation of solvents, the crude product was distilled under vacuum. Acetates 9 were prepared according to the procedure described for acetates 6. REFERENCES (1) W. H. Brown and H. Sawitzky, Can. J. Chem., 34, 1147 (1956). (2) S. Arctander, Perfume and Flavor Chemicals (Montclair, NJ, 1969). (3) German Patent DE 3 527 975 (1987). (4) Y. K. Yuriev and N. S. Zefirov, Zh. Obshch. Khim., 30, 1150 (1960). (5) Y. K. Yuriev and N. S. Zefirov, Zh. Obshch. Khim., 33, 411 (1963).
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